CHEM 332- Fall 2012

Online Lab Handouts:

• Introduction to Microscale
• Lab 1: Reduction of Vanillin using sodium borohydride
• Lab 2: Oxidation of Cyclohexene to form Adipic Acid
• Lab 3: Formation of Benzoic Acid via Grignard addition
• Lab 4a: Synthesis of Lidocaine - Part I - Acyl Substitution Reaction
• Lab 4b: Synthesis of Lidocaine - Part II - an S_N2 reaction
• Lab 5: Formation of Isobutyl Propionate - an Esterification reaction
• Lab 6: Friedel-Crafts Alkylation of para-Xylene
• Lab 7: Qualitative Analysis Lab - Identification of an Unknown Compound
• Appendix A - Microscale Apparatus Set-ups

Spectroscopy Information:

• Infrared Spectroscopy
• Example Spectra
• IR Practice Problems
• Mass Spectroscopy
• Sample Spectra - Examples, Problems
• Proton Nuclear Magnetic Resonance Spectroscopy
• Proton NMR Examples
• Proton Integration Info
• IR and Proton NMR Problems
• Carbon-13 Nuclear Magnetic Resonance Spectroscopy
• Example Spectra
• Spectroscopy Problems - IR, Proton NMR, Carbon NMR