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Chemistry 210, Section 001, 002, and
003 Spring, 2006 Introduction To Analytical Chemistry |
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Instructor:
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Dr. Joseph Topping Smith Hall, Room 555 Phone: 410-704-3056 Fax: 410-704-4265 e-mail: jtopping@towson.edu |
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Office Hours: |
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Tuesday and Thursday @ 9:00-9:30 PM and
Monday @ 9:30-11:00 AM |
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Lecture: |
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9:30-10:45 AM, Tuesday and Thursday in
Smith 524 |
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Laboratory: |
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Lab lecture will precede most (but not
all) laboratory sessions and sections 001 (Tuesday) and 002 (Thursday) will
meet in Smith 554 @ 1:00 PM; Section 003 (Monday) will meet for lab lecture @ 1:30 in
Smith 508. All laboratory work will take place in Smith 509 and connecting
rooms and will begin at the completion of lab lecture. Lab closes @ 5:00 PM
on Tuesday and Thursday and 5:30 PM on Monday. You are free to attend any lab
session other than your own, if you fall behind and need extra time, but you
are expected to faithfully attend your assigned section each week. |
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Required Texts: |
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Exploring Chemical Analysis, 3rd
Edition D. Harris, W. H. Freeman Publishers,
2005; ISBN 0-7167-0571-0 You may wish to purchase the Solutions
Manual For Exploring Chemical Analysis; ISBN # 0-7167-1170-2 |
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Other Required Materials: |
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Safety Glasses for Laboratory and a
Laboratory Notebook that has numbered pages and makes carbon copies. |
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Grading: |
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There will be four hour exams and a
final exam. Each is of equal value and
the four highest scores will count as 64% (16% per exam) of the total
grade. The remaining 36% will be based
on laboratory performance (laboratory reports and the instructor’s evaluation
of your general competence in laboratory.) The +/-
grading system will be used. |
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Grading Standards: |
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ABCDF |
88% and above 78% - 87% 68% - 77% 58% - 67% 57% and below |
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Make-Up Exams: |
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There
are none; a missed exam automatically becomes the lowest score and the score that
is dropped (see section on grading, above.) |
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Attendance: |
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Lecture – Mandatory only
for exams. Laboratory – Students
must complete all experiments, including an acceptable notebook record and
reports for all experiments. |
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Cheating: |
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Cheating on an exam or
laboratory report will result in a zero for that particular experience. |
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Lecture Outline: |
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The Analytical Process Chemical Measurements Math Toolkit Statistics Hour Exam I Quality Assurance Gravimetric Analysis Titration Acids and Bases Hour Exam II Acid-Base Titrations Polyprotic Acids and Bases Chemical Equilibrium Hour Exam III Optical Methods Atomic and Molecular Spectrophotometry Principles of
Chromatography Gas and Liquid
Chromatography Hour Exam IV Final Exam…Comprehensive,
one question from each chapter. |
Laboratory
Schedule:
The Analytical Balance:
Determining the Need for Drying Samples
Precision and Accuracy of Pipets and Volumetric Flasks
Gravimetric and
Volumetric Determinations of Chloride (A comparison of
analytical methods)
Acid-Base Titrations
Complex-Forming Titration (Alternate
approaches to the determination of calcium
In hard water)
Determination of the Dissociation Constant
of a Weak Acid Using UV/Visible
Spectrophotometry
Separation and Analysis of a Mixture
Using High Performance Liquid
Chromatography and UV/Visible Spectrophotometry
Atomic Absorption and Emission
Spectroscopy (Determination of trace metals)